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Duplicate Sample: To determine the reproducibility of the procedure within the same experiment or batch on analysis

Alshehri T, Wang J, Singerling SA, Gigault J, Webster JP, Matiasek SJ, Alpers CN, Baalousha M (2023) Wildland-urban interface fire ashes as a major source of incidental nanomaterials

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One-dimensional temperature program: the initial temperature for all four cuts is 45 C (held for 2 min), and then it is raised at a rate of 6 C/min, reaching 93 C for cut 1, 132.6 C for cut 2, 174 C for cut 3, and 216 C for cut 4, followed by a rapid cooling to 60 C (for cuts 1 and 2) or 80 C (for cuts 3 and 4)